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Full Record Details
Persistent URL
http://purl.org/net/epubs/work/50659
Record Status
Checked
Record Id
50659
Title
Neutron diffraction, electronic band structure, and electrical resistivity of Mo
3-x
Ru
x
Sb
7
Contributors
C Candolfi (ENSMN)
,
B Lenoir (ENSMN)
,
J Leszczynski (ENSMN)
,
A Dauschert (ENSMN)
,
J Tobola (AGH U., Krakow)
,
SJ Clarke (Oxford U.)
,
RI Smith (STFC Rutherford Appleton Lab.)
Abstract
Neutron diffraction experiments and Korringa-Kohn-Rostoker with coherent potential approximation electronic band structure calculations as well as electrical resistivity measurements have been performed on polycrystalline Mo3-xRuxSb7 samples for 0 <= x <= 1. Neutron diffraction studies have been undertaken at room temperature and extended down to 4 K to get a better understanding of the crystalline structure modifications as the Ru content increases. Both structural and chemical characterizations have unambiguously revealed a solubility limit of the Ru atoms close to 0.8. Electronic band structure calculations have provided theoretical evidence of a progressive transition from a metalliclike state (x = 0) toward a semiconducting-like character as x = 1 is approached, although the solubility limit of Ru precludes a crossover to a semiconducting behavior. The theoretical prediction has been experimentally confirmed by low-temperature electrical resistivity measurements from 2 up to 350K.
Organisation
ISIS
,
ISIS-POLARIS
,
STFC
Keywords
Materials
,
Chemistry
Funding Information
Related Research Object(s):
Licence Information:
Language
English (EN)
Type
Details
URI(s)
Local file(s)
Year
Journal Article
Inorg Chem
48, no. 12 (2009): 5216-5223.
doi:10.1021/ic900171u
2009
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