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Full Record Details
Persistent URL
http://purl.org/net/epubs/work/54386
Record Status
Checked
Record Id
54386
Title
New high temperature gas flow cell developed at ISIS
Contributors
R Haynes (STFC Rutherford Appleton Lab.)
,
ST Norberg (STFC Rutherford Appleton Lab.)
,
SG Eriksson (Chalmers U., Sweden)
,
MAH Chowdhury (STFC Rutherford Appleton Lab.)
,
CM Goodway (STFC Rutherford Appleton Lab.)
,
GD Howells (STFC Rutherford Appleton Lab.)
,
O Kirichek (STFC Rutherford Appleton Lab.)
,
S Hull (STFC Rutherford Appleton Lab.)
Abstract
A flow-through quartz gas cell, together with a gas flow control and monitoring system, has been designed and constructed at ISIS. This equipment allows neutron powder diffraction data to be collected on samples at temperatures up to around 1300 K when exposed to user chosen mixtures of O2, Ar, CO2, and CO. By exploiting the sensitivity of neutrons to the presence of light atoms such as oxygen, it is possible to probe the crystal structure of oxide materials as a function of oxygen partial pressures down to log10p(O2) of about -20. The resultant structural information can then be correlated with the bulk properties of the materials, whose research and technological interests lie in fields such as energy production, storage materials, catalysis, and earth science.
Organisation
ISIS
,
ISIS-POLARIS
,
STFC
Keywords
Materials
,
high temperature
,
gas flow cell
,
SSTD 2010-2011
Funding Information
Related Research Object(s):
Licence Information:
Language
English (EN)
Type
Details
URI(s)
Local file(s)
Year
Journal Article
J Phys Conf Ser
251 (2010): 012090. Presented at: International Conference on Neutron Scattering 2009 (ICNS 2009).
10.1088/1742-6596/251/1/012090
2010
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